VISCOSITY LABORATORY
         
      Quantity
      Dynamic viscosity is a derived physical quantity which defines a resistance at liquid flow. Dynamic viscosity is defined as a ratio of shear stress to shear rate. Kinematic viscosity is defines as a ratio of the dynamic viscosity to density.
      Unit - dynamic viscosity: Pa·s; kinematic viscosity: m2·s-1.
      Tasks of the laboratory
      The main tasks of the laboratory are research and development for the realisation and dissemination of the unit of viscosity. 
      International comparisons
      ASTM Project D.02.07.A
DUNAMET Project No. D22
EUROMET Project No. 415 - EUROMET.M.V-K3 - key comparison.

       
    Available metrological services
     
Calibration or Measurement services Viscosity  Range Expanded uncertainty (k=2)
Standard Capillary Viscometers (0,001 - 100) mm2·s-2 (0,1 - 0,3) % 
Falling Ball Viscometers (0,6 - 150 000) mPa·s (0,5 - 2,0) %
Rotational Viscometer (0,6 - 1 500 000) mPa·s (0,5 - 3,0) %
CRM Liquids (2 - 100 000) mm2·s-1 (0,2 - 1,0) %
      Methods of measurement:
      The primary standards are calibrated by the step-up method, using the value of the kinematic viscosity of the redistilled water at temperature of 20 °C. The viscometers of higher nominal values are calibrated by direct comparison with viscometers of lower nominal value. 
The lower order standards and working instruments (capillary viscometers) are calibrated by the direct comparison with SMU standard viscometers.
Falling Ball and Rotational Viscometers are calibrated by using of certified reference liquids which are traced to the national standard of viscosity.
       
    Instruments in use
     


Viscosity standard bath

The National standard consists of two sets of Ubbelohde capillary viscometers with 500 mm capillary length and two sets of Ubbelohde capillary viscometers with 400 mm capillary length. The measurement device consists of temperature controlled bath with accesories (heating circulator and immersion cooler), Pt25 thermometer, device for water preparation (reference liquid for derivation of scale of kinematic viscosity), computer controlled automatic measuring device for efflux time measurement and measurement control. The standard device is computer operated and process of measurement is free programmable and fully automated by the set of bistabil electromagnetic valves (four valves for each of 8 viscometers in the bath).

The efflux time measurement is realized by swiching on/off the counter, when liquid level passes by the position of optical sensors. Sensors position is adjustable to coincide with ring marks of viscometer.
         
     
Contact
Mr. Dušan Trochta
phone: + 421 2 60294 214
e-mail: trochta@smu.gov.sk